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  1. Given are the following spectra. a. Determine the degree of unsaturation for the compound. b. Assign five pertinent peaks in the IR spectrum. c. Suggest a structure for compound W based on the spectra given. Show all your work and clearly indicate what your final answer is.

  2. The following exercises are designed to help you become familiar with predicting the 1H NMR spectra of simple organic molecules. For each example you should find the number of signals you expect, where they should show on the scale (chemical shift), and what shape they should be (splitting patterns).

  3. Winter 2016. (Problems from former Chem 30BL finals) 1. Compound W has an empirical formula of C11H10O2. Given are the following spectra. Show all your work (= label peaks in the spectra!) Determine the degree of unsaturation for the compound. Assign the six pertinent peaks in the infrared spectrum.

  4. NMR Practice Problems. In the following examples, we will learn how to solve NMR practice problems step-by-step in over 100 min video solutions which is essential for organic structure determination.

  5. Chemistry 233 Chapter 13: NMR Spectroscopy Problem Set. 1) For each compound below, identify each chemically distinct type of hydrogen. Specify the number of 1H NMR signals you would expect to see. Tips: 3) Consider the indicated protons in each of the three compounds below.

  6. This site provides one dimensional spectra of different nuclei, COSY, HSQC, HMBC and some less common spectra of various compounds for you to interpret, together with worked solutions. Hopefully, these problems will provide a useful resource to help you better understand NMR spectral interpretation. Legacy notice.

  7. NMR Practice Problems. Tell precisely how you would use the proton NMR spectra to distinguish between the following pairs of compounds: 1-bromopropane and 2-bromopropane. propanal and propanone. ethyl acetate (MeCO2Et) and methyl propanoate (EtCO2Me) 1-butyne and 2-butyne.

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